Download 30 paintings by Marc Chagall PDF

By Marc Chagall

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B. Fe(bipY)3 26l und Zn(biPY)3 2$, sind einander ähnlich. Monoprotoniertes Bipyridin absorbiert bei 303 nm (Bande I) und 243 nm (Bande 11), während das Dikation nur eine AbsOl;ptionsbande bei 290 nm zeigt. Das Auftreten der Farbe in den Komplexen ist auf einen erlaubten t2g-n*-Übergang zurückzuführen 71). ), während in polaren Lösungsmitteln für mono- und diprotonierte Bipyridine eine transoide ske~Konformation (Interplanar-Winkel 25-30') gefunden wurde. 1 Bipyridin 37 allerdings tritt eine Hochfeld-Verschiebung der Wasserstoffatome in a-Position zum Stickstoffatom um ca.

Am Anfang der Komplexchemie standen anorganische Komplexe, aber es zeigte sich, daß auch organische Moleküle befähigt sind, stabile Komplexe zu bilden. 7 Komplexierungsvermögen des 2,2'-Bipyridins und seiner Abkömmlinge Seit der Entdeckung des 2,2'-Bipyridins als Nachweisreagens für zweiwertiges Eisen 1) sind viele seiner Derivate auf ihre Schwermetall-Komplexierung untersucht worden. Ihr starkes Komplexierungsvermögen wird durch den Chelateffekt und die besondere elektronische Struktur der Liganden gesteuert.

1 Bipyridin 33 Obwohl die Nickelkomplexe 23 und 24 die gleiche Anzahl an analogen Donorzentren enthalten, findet man einen groBen Unterschied der Komplexbildungskonstanten (K). Dieser beim übergang von 23 zu 24 auffallende "Chelateffekt" läßt sich thermodynamisch begründen, da die Komplexbildungskonstante K nach Gleichung (1) mit der freien Enthalpie 6G verknüpft ist: In K =- 6G (1) RT Diese steht mit der Enthalpie 6H und der Entropie 6S im Zusammenhang: 6G = 6H - T6S (2) ( Gibbs-Helmholtz-Gleichung) Daraus folgt: In K 6H RT + 6S R (3) Die Entropie, Maß für die Unordnung eines Systems, nimmt nach Anlagerung eines zweizähnigen Liganden zu, denn bei jeder Substitution werden zwei Lösungsmittelmoleküle vom Zentralion verdrängt, so daß nach der Umsetzung die Zahl der unabhängig voneinander beweglichen Teilchen größer ist.

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